Friday, 22 January 2021

XI BIO LAB WORK-Pigment separation by using paper chromatography

 


 Procedure

  • Take a few freshly plucked green spinach leaves.

  • Using scissors,  cut the spinach leaves into small pieces and let them fall into the mortar.

  • Take a measuring cylinder that contains 5ml of acetone and pour it into the mortar.

  • Grind the spinach leaves using the mortar and pestle.

  • Place the extract into a watch glass using a spatula.

  • Take a strip of filter paper having a narrow notch at one end of the strip.

  • Take a pencil and a scale and draw a horizontal line with a pencil about 2-3 cm away from the tip of the notch.

  • Put a drop of the pigment extract in the middle of the line with the help of a capillary tube.

  • Allow the drop to dry and repeat till four or five drops are placed on the paper.

  • Take the chromatographic chamber and pour ether acetone solvent in it.

  • Fold one end of the filter paper strip and staple it.

  • Using a thread, hang the filter paper strip in the chromatographic chamber.

  • The loading spot should remain about 1 cm above the solvent level.

  • Leave the chromatographic chamber undisturbed for some time.

  • We can observe, as the solvent moves through the paper, it spreads the different pigments of the mixture to various distances.

  • When the solvent rises about 3/4th up the strip, remove the strip carefully and let it dry.

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